Universal X-ray diffractometer D5000 (Siemens)
- Vertical circular goniometer with Bragg-Brentano focusing principle
Technical details:
Primary beam path:
- X-ray tube with Cu anode and line focus
- Soller collimator
- Gap diaphragm
- Irradiated area 4 mm × 12 mm
Secondary beam path:
- Boundary blind
- Soller collimator
- Gap diaphragm
- Curved graphite single crystal monochromator
- Scintillation counter tube
Angle range:
- 0° ≤ 2 θ ≤ 150° (minimum step size 2 θ = 0.002°)
Sample request:
- crystalline (compact, powdery)
Surface condition of the samples:
- just
Sample dimensions:
- 4 mm … 10 cm × 12 mm … 10cm × ≤ 15 mm
Software package:
- Diffrac plus (BRUKER AXS) with various evaluation modules
Phase analysis:
(qualitative/quantitative)
- EVA with PDF-2 database
- TOPAS with structural data files
